Determination of Aluminum in Dialysis Concentrates by Atomic Absorption Spectrometry after Coprecipitation with Lanthanum Phosphate

AuthorEmine Kılıçkaya Selvien
AuthorUğur Şahinen
AuthorSerkan Şahanen
Issued Date2017-07-31en
AbstractThis method was developed for the determination of trace amounts of aluminum(III) in dialysis concentrates using atomic absorption spectrometry after coprecipitation with lanthanum phosphate. The analytical parameters that influenced the quantitative coprecipitation of analyte including amount of lanthanum, amount of phosfate, pH and duration time were optimized. The % recoveries of the analyte ion were in the range of 95-105 % with limit of detection (3s) of 0.5 µg l-1. Preconcentration factor was found as 1000 and Relative Standard Deviation (RSD) % value obtained from model solutions was 2.5% for 0.02 mg L-1. The accuracy of the method was evaluated with standard reference material (CWW-TMD Waste Water). The method was also applied to most concentrated acidic and basic dialysis concentrates with satisfactory results.en
DOIhttps://doi.org/10.22037/ijpr.2017.2079en
KeywordAluminumen
KeywordLanthanium phosphateen
KeywordCoprecipitationen
KeywordDialysis concentrateen
KeywordAtomic absorption spectrometeren
PublisherBrieflandsen
TitleDetermination of Aluminum in Dialysis Concentrates by Atomic Absorption Spectrometry after Coprecipitation with Lanthanum Phosphateen
TypeOriginal Articleen

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